GOVERNMENT OF THE PUNJAB
EXCISE AND TAXATION DEPARTMENT
THE PUNJAB DISTILLERY RULES
PRELIMINARY NOTIFICATION
[21st Feb,
1998]
Notification No. 13-98/161-EX(P)III, dated 21st February, 1998.
Excise Commissioner, Punjab.
9.0 In these rules unless a different
intention appears from the subject or context:-
(a)
“License” mean a license granted for a distillery under
section 21 of the Punjab Excise Act 1 of 1914.
(b)
“AETO” includes E&T Inspector.
(c)
“Wash” means a saccharine solution from which after
distillation, spirit is obtained.
(d)
“Bub” is a composition itself in a state of
fermentation prepared, for addition to wash, to promote fermentation.
(e)
“Low wines” means impure spirits produced from the
first distillation of the wash in a pot still.
(f)
“Feints” means that portion of the distillate from the
low wines which is considered unfit by reason of its impurities to be collected
in the spirit receiver.
(g)
“Spirit” means both finished and unfinished spirit.
(h)
“Rectified spirit” means spirit of a strength of 43
degrees or more over-proof.
(i)
“Receiver” means any vessel into which the worm of a
still discharges.
(j)
“Spent wash” means the residue left after the wash has
been exhausted of spirit.
(k)
“Spent lees” means the residue left after unfinished
spirit has been redistilled.
(l)
“Spiced spirit” means spirit redistilled after the
addition of flavours and spices to plain spirit.
(m)
“Special spiced spirit” means spiced spirit approved by
the Excise Commissioner for issue as special spiced spirit. It includes matured
spirit more than two years old.
(n)
“Malt Whisky” means whisky manufactured from malt only
or blend of such whisky with plain spirit in such a ratio that plain spirit
does not exceed one third thereof, [“Light Malt Whisky”
means a blend of minimum of 20% whisky manufactured from malt with plain spirit
which does not fall within the definition of malt whisky”].
(o)
“Matured Whisky” means whisky matured in wood for a
period of not less than two years.
(p)
“Distillation” includes reinstallation.
(q)
“Excise and Taxation Officer” means the Excise and
Taxation Officer incharge of a distillery or having jurisdiction in the area
where a distillery is sought to be located.
Grant of License
9.1 The Excise
Commissioner has full power to grant or refuse applications for licenses with
reference to the requirements of the province.
9.2 Any person
desiring to obtain a license for a distillery under section 21 of the Punjab
Excise Act (1 of 1914) may apply to the Collector through the Excise and
Taxation Officer.
9.3 Every
application for a license for a distillery shall be in writing in the form D.1
and shall be accompanied by:-
(a)
a correct plan of the premises which the applicant
proposes to use for the purposes of his business under his license and of the
building existing or to be erected thereon, for the said purposes.
(b)
A list and plans of all warehouse store rooms and other
places appertaining thereto, or to be used in connection therewith; and
(c)
A certificate from the Civil Surgeon that there is no
objection on sanitary grounds to the construction of distilling premises, or to
the distillation of spirit on the site and in the building shown in the
accompanying plans.
9.4 No licence shall be granted unless
and until the applicant therefore has:-
(a)
deposited as security for the fulfillment of all the
condition of his license a sum to be fixed by the Excise Commissioner which
shall not be less than Rs. 2000/- or more than Rs. 5000/- in amount; and
(b)
satisfied the Collector, that the proposed buildings plant
and apparatus to be used in connection with the business of distillation,
storage and issue of spirit are built in accordance with the prescribed
regulations and that due precaution has been taken against fire; but in respect
of the present buildings, plant and apparatus of existing distilleries which do
not conform with the provisions of these rules, the Excise Commissioner may in
writing, grant exemption from the operation of any of these rules.
9.5 The license
shall be in form D.2 and is not transferable except with the sanction of the
Excise Commissioner.
Security
9.6 The licensee
shall execute a bond in the prescribed form pledging the premises, stock of
spirit, stills all apparatus and utensils employed in the manufacture and
storage of spirit for the due discharge of all payments which may become due to
Government, with the sanction of the Excise Commissioner the licensee may in
lieu of executing such a bond deposit Government promissory notes of such value
as the Excise Commissioner may direct. A deposit made under this rule shall be
separate and distinct from the security deposit required by rule 9.4.
Period of Licenses
9.7 Licenses are
granted without limit of the period for which they are in force but can be
canceled for breach of the terms, or can be determined by the Excise
Commissioner after one year’s notice.
9.8 If the
licensee ceases to work the distillery without giving notice as required in his
license, or if he ceases to work the distillery within the period of such
notice, the Collector may take possession of the distillery and its plants and
work it by himself or by the agency of any person authorized by him in that
behalf for a period equivalent to the period of notice or unexpired period of
notice as the case may be.
9.9 In the case mentioned
in the foregoing rule the licensee shall be entitled to receive from Government
such reasonable rent for the use of the buildings and plant as shall be
determined by the Excise Commissioner.
9.10 If a license
be revoked, canceled or determined the licensee shall dispose under the
conditions of his license his stock of spirit, apparatus, storage vessels and
other distilling plant in such manner as the Excise Commissioner may direct.
9.11 The licensee
may not hypothecate the whole or any part of the licensed premises without the
previous written sanction of the Excise Commissioner.
Inspection
9.12 The licensee
shall at any time permit the Collector or any other officer authorized by the
Collector in that behalf, to inspect and examine his licensed distillery, the
premises and warehouses connected therewith and the spirit made and stored
therein, and shall render to the Collector or officer (as aforesaid) all proper
assistance in making such inspection and examination.
9.13 The licensee
shall agree to the posting of a Government excise establishment to his
distillery for the purpose of ensuring the due observance of these rules and
for watch and ward. This establishment shall consist of an AETO and as many
E&T Inspectors and constables as the Excise Commissioner shall deem
sufficient for the requirements of the distillery. This staff, subject to the
general orders of the collector or other higher authority shall be under the
control of the Excise and Taxation Officer.
9.14 The licensee
shall provide within his distillery enclosure an office for the AETO as well as
quarters, to be approved by the Director Excise and Taxation for the AETO and
constables who will be required to remain within the distillery enclosure on
night duty.
9.15 The licensee
shall if required by the Excise Commissioner provide residential quarters for
the Government excise establishment posted to the distillery.
9.16 The
licensee shall pay a fee comprising:-
(i)
the charges on account of salaries (including leave and
pension contributions) of the excise establishment posted to the distillery in
pursuance of the provisions of rule 13
payable into the Government treasury by the 15th of the month of which the charges relate; and
(ii)
[Rs. 50,000.00] per
annum payable within 15 days of the commencement of the financial year, or in
case of the grant of a new license, within 15 days of such grant.
9.17
The licensee shall when required permit samples of
the materials used or spirit prepared in the distillery to be taken for
analysis under the orders of the Collector or the Excise Commissioner, by an
officer authorized by them to take samples, or by the Excise and Taxation
Officer or the AETO, Each sample shall be taken in three reputed quart bottles
or (when the materials cannot be placed in bottles) in three parcels, in the
presence of the licensee or a responsible representative deputed by him for
this purpose; each bottle or parcel shall be immediately and securely sealed in
the presence of the AETO and the licensee or his representative. Both of them shall
sign a label which shall be affixed to the bottle or parcel and describe the
contents thereof as accurately as possible. One bottle or parcel shall then be
made over to the licensee’s representative, the second shall be sent for
analysis and the third retained by officer concerned pending the disposal of
the case.
9.18
The licensee shall afford all reasonable assistance
to the AETO in carrying out his duties.
9.19
The licensee unless he personally acts as manager,
shall be bound to appoint a competent manager as his agent, whose appointment
shall be subject to the approval of the Director Excise and Taxation.
9.20
The licensee shall furnish to the Excise and
Taxation Officer a list containing the names of any manager or assistant
manager employed by him and of all employees whose duties require them to enter
the distillery enclosure. The Excise and Taxation Officer shall forward a copy
of this list to the Collector and the licensee shall not employ on such duties
persons to whom the Collector objects.
9.20-A Under rule
5.39 (29) (a) (iv) of the Punjab Excise Manual, Volume II as amended vide
Excise Department Notification No.2318.Ex dated the 25th September, 1953 a
liquor licensee cannot, unless otherwise permitted by the Excise Commissioner
sell Pakistan Made Foreign spirit except in bottles of the following sizes;-
(a)
reputed quart bottles of the capacity of 26-2/3 Ozs.
(b)
Reputed pint bottles of the capacity or 13-1/3 Ozs.
(c)
Quarter bottles of the capacity of 6-2/3 Ozs.
The capacities of
bottle, in which Pakistan Made Foreign spirit manufactured in East Bengal is
permitted to be bottled and sold have been fixed, vide rule 247 (a) and (b) of
the reprint under the Bengal Excise Act to range from 22 Ozs. And 11 Ozs to
12/2 Ozs. respectively in the case of quarter and pints of whisky, brandy and
rum, and 22 Ozs and 11 Ozs to 12 Ozs respectively in the case of quarts and
pints of gin. Accordingly, as imported from East Bengal will be exempt from the
operation of the aforesaid rule. This exemption will, however, be subject to
the following conditions:(a) That only quarts and pints will be imported from
East Bengal.
(b)
That the minimum guaranteed quantity of its contents
shall be clearly indicated on the label in conspicuous letters and figures.
(c)
That six quarts or one dozen pints of spirit imported
from East Bengal shall be treated as
equivalent to one Imperial gallon for purposes of levy of duty under order 2.1
of the Punjab Excise Manual Volume II read with para 3.22 ( g) of the Punjab
Excise Manual Volume III.
(d)
That vend fee shall be recovered treating these bottles
to be reputed quarts and pints within the meaning of the Punjab Excise Act (i.e
six quarts of one dozen) for purposes of recovery of vend fee, in terms of rule
5.31 of the Punjab Excise Manual Volume II.
(e)
That one quart or two pints of any kind of spirit
imported from East Bengal shall be deemed to comprise one unit of liquor under
the, Punjab Prohibition and Restriction of liquor Rules, 1949.
(Vide Excise Commissioner’s
circular memorandum No.2512/EX dated the 20th October, 1953).
9.21
If the licensee desires to employ any person
temporarily for duties requiring him to enter the distillery, e.g to replace a
servant who is absent on leave or for sickness otherwise or to perform any
special duty in the distillery, he shall inform the Inspector, who shall add
the name of such person to the list mentioned in rule 9.20 above.
9.22
If any servant leaves the service of the licensee
or is not longer employed in duties requiring him to enter the distillery, the
licensee shall give notice to the Inspector and have his name removed from the
list. The Inspector shall inform the Collector accordingly.
9.23
No person shall be allowed to the distillery except
the licensee, any director of a company owning the distillery, any Government
official or police officer whose duties require him to enter the distillery any
person introduced by the licensee or director, the manager and any person whose
name has been entered on the list mentioned in rule 9.20 above.
9.24
Every person entering the distillery shall on
leaving the distillery be liable to be searched under the AETO’s order, but the
AETO shall not have any person searched, except upon reasonable grounds for
suspicious and he shall record in his diary the details of every search made.
9.25
The licensee shall not close the distillery for
more than three days in any month, exclusive of Sundays and holidays, without
the previous written permission of the Collector.
THE COMMENCEMENT AND CLOSURE OF DISTILLERY
WORK AND WORKING ARRANGEMENTS
9.26
If it is intended to close the distillery for a
period of 15 days or more, the licensee shall give notice in writing to the
Collector of his intention not less than 15 days prior to the date on which it
is intended to close.
9.27
Before a distillery commences work or recommences
work after a closure of 15 days or more, the licensee shall give notice, in
writing to the Collector at least 10 days prior to the date fixed for the
commencement or recommencement of work.
9.28
The ordinary working hours of a distillery shall be
as follows:-
SUMMER (16TH APRIL TO 15TH SEPTEMBER
All working
days except Fridays. From 7.0 A.M
to 4.0 P.M with an interval of one
hour from 12 noon to 1.P.M.
Fridays
From 7.A.M to12 Noon.
WINTER (16TH LSEPTEMEBER
TO 15TH APRIL
All working days except Friday From 7.30 A.M to 4.0 P.M (with an
interval from
12.30 P.M to 1.0 P.M ).
Fridays From 7.30 A.M to 12.30 P.M
(without any interval
9.29 During the ordinary working hours, if
the distillery is working, the outer door shall, except as provided in rule
9.33 below, be kept continually unlocked.
9.30 Upon giving
a general notice to the AETO, or if night work is only occasionally, upon
giving notice to the AETO not less than four hours before the ordinary closing
hours of the day after which night working is to be done, the distillery may be
worked at hours other than the ordinary working hours.
9.31 If stills in
any distillery are so worked that there is ordinarily no period on any ordinary
working day in each week during which the stills are simultaneously silent, the
licensee shall at which once a week on any day other than a Sunday or a holiday
gazetted under the Negotiable Instruments Act and at any time during the
ordinary working hours by day, after giving to the AETO 24 hours notice of the
day and hour fixed by him, work off every still in the distillery and arrange
that no distillation shall be in progress for one hour in order that the AETO
may take an account of the working of the distillery.
9.32 A distillery
may remain open for work on a Sunday or a holiday gazetted under the Negotiable
Instruments Act provided notice is given to the Distillery AETO at least 24
hours before the Sunday or holiday in question and a fee shall be paid to
Government not exceeding Rs. 15 per day or part of a day as fixed by the Excise
Commissioner for each distillery. If a distillery remains open for working
after due notice to the Distillery AETO on any of the holidays specified below,
the fee payable to Government for every such holiday shall be double the
ordinary fee:-
(1)
Jumatul-Wida
(2)
d-ul-Fitr (Principal day)
(3)
Id-ul-Azha (Principal day)
(4)
Muharram (Tenth day)
(5)
Pakistan day
(6)
Quaid-i-Azam Death Anniversary.
(7)
Id-I-Milad-un-Nabi
(8)
Qaid-I-Azam’s Birth day and Charismas day.
If the distillery remains open for the fermentation of but
and wash only the fee payable shall be one third of the ordinary fee.
Explanation.- “Open
for work” shall mean any normal operation connected with the distilling and
bottling of spirit and includes the fermentation of bub or wash.
9.32-A An account
of overtime fee charged under rule 9.32 above shall be maintained in the distillery
register in form D23, and the amount due for each month shall be payable within
seven days of the closure of the month
concerned. Intimation as regards the amount due during the month shall be sent
by the Distillery AETO to the Manger of the Distillery at the close of each
month.
9.33 If the
distillery work at other than the ordinary hours by day, the Inspector shall
remain present within the distillery enclosure, but except incase of emergency,
the licensee shall not require him to lock or unlock any receiver, at or other
part of the plant; and he shall lock the outer door of the distillery, and
shall not allow any person to enter or leave the distillery enclosure, except
in accordance with the arrangements to be made with the sanction of the Collector
for the convenience of persons who may be permitted to enter or leave the
distillery at fixed hours, in connection with the operation being carried on.
9.33-A If the
distillery works on Sunday or a gazetted holiday, the AETO shall remain present
for duty within the distillery enclosure but unless so authorized by the
Collector, he shall not be required to take any action for the bottling or
issue of spirit and he shall lock the outer door of the distillery and shall
not allow any person to enter or leave the distillery enclosure, except in
accordance with the arrangements to be made with the sanction of the Collector
for the convenience of persons who may be permitted to enter or leave the
distillery at fixed hours, in connection with the operation being carried on.
9.34 (1)
The use of naked lights of any description within the distillery is
prohibited.
(2) Smoking in
any portion of the excise enclosure where spirit is manufactured, stored behold
or issued is strictly prohibited.
PRESCRIBED OUTTERNS OF SPIRIT AND STOCKS OF SPIRIT AND DISTILLING BASE.
9.35 The licensee
shall if there is a demand upon his distillery for such a quantity, produce
during each colander year at least 90 percent of the outturn of spirit which
his stills are capable of producing according to the estimate of their charge
capacity entered in his licence. The calculation of the outturn shall be based
on the assumption that 100 gallons of wash, whether or gur, molasses or mahua
will yield 12 proff gallons of spirit, that each continuous still will work on
an average 12 hours a day and that each pot still will be charged with wash one
and a half times a day and that stills will work for an average of five days a
week throughout the year.
9.36 Subject to
the provisions of the preceding clause, the licensee shall maintain a stock of
spirit, bulk as well as bottled, so that such stock shall, at the beginning of
each month from May to September inclusive, after allowing for compliance with
all orders in hand at the time be equal to one third the average amount issued
during that month in the three preceding years and at the beginning of every
other month to half such average amount. If on account of any emergent and
unexpected demand during the last days of the preceding month, the stock on the
first day of any month is below the amount required by this clause, the
licensee shall, in the beginning of the month make it good with the least
possible delay. In case of serious or continued failure to comply with this
conditions the licensee may be required to pay a penalty determined by the
Excise Commissioner and persistent failure to comply with this condition will
entail the cancellation of the licensees license.
9.37 The licensee
shall have always in stock, in a gur, molasses, or mahua store, to be provided
by him and approved by the Excise Commissioner a quantity of gur, molasses or
mahua, sufficient for the preparation of wash for the full working of all his
stills, calculated upon the data set forth in rule 9.35 above for 10 full
working days in the months from October to March inclusive to April to
September. The stock shall be calculated on the basis that it requires 3 maunds
of gur or four maunds of molasses or mahua to prepare 100 gallons of wash,
provided that if the licensee maintains a stock of spirit over and above the
quantity required by rule 9.36 above, then the stock of gur, molasses or mahua
may be correspondingly reduced. In making this calculation one maund of gur,
molanesor to LPG of molasses or spirit respectively. The licensee shall on the
1st and 15th day of each month,
report to the AETO the quantity then in stock and shall permit the AETO to
verify the quantity if he desires to do so.
9.37-A The
licensee shall always have in stock empty quart, pint and half pint bottles,
pale as well as dark, so that after complying with all orders in hand, the
stock of empty bottles shall be equal to the amount of bottles issued during
the corresponding month of the last year. The licensee shall on the 1st and 15th day of each month,
report to the Inspector the quantity of empty bottles, in gross numbers then in
stock, and shall permit the Inspector to verify the said quantity if he desires
to do so.
ACCOUNTS AND REGISTERS
9.38 The licensee
shall keep up the registers which are by these rules prescribed for maintenance
by the licensee, and shall submit them for inspection when required.
9.39 The licensee
is entitled to inspect those registers maintained by the AETO which relate to
the operation of distillation and issue and to stock-taking and notice should
be given to him of any corrections made in them.
9.40 (1) If the
licensee has a laboratory attached to his distillery and requires spirit for
use in the laboratory he shall be entitled to remove to the laboratory from the
distillery duty free, from either the safes of the stills, the spirit receivers
the spirit store or from the maturing warehouse, finished spirit and unfinished
spirit to the extent of three gallons per month provided that not more than two
quart bottles shall be so removed at any time and the spirit so removed shall
not be used in the distillery laboratory otherwise than for experimental work
connected with distillery operations only. The licensee shall keep a regular
account of the disposal of such duty free spirit which will be subject to
examination by excise officers. All spirit which comes waste in the laboratory
and does not by the addition of any chemicals or otherwise become deleterious
shall be returned to the distillery for re-distillation
(2)
As application for every quantity of spirit required to
be removed from the distillery under the rule must be made in writing to the
Distillery AETO, who shall record thereon the quantity and strength of the
spirit taken, and make a note of the same in his diary and other relevant distillery
registers.
(3)
If spirit removed under the concession is used
otherwise than as permitted by subrule (1) of this rule, the concession may be
withdrawn.
9.40-A The
licensee shall also be entitled to remove once a year duty free Pakistan made
foreign liquor and country spirit not exceeding one gallon or with the
permission previously obtained of the Excise Commissioner in specified
quantities in excess of one gallon from the distillery for laboratory
examination in a foreign country; provided that he shall keep a regular account
of the disposal of such duty free spirit, which will be subject to examination
by Excise officers. He shall also produce within six months the customs receipt
in respect of the duty paid on such consignment on its entry into a foreign
country. In default the licensee shall be required to make good the duty which
otherwise would have been levied on the quantity of liquor when it left the
distillery. The licensee shall, if required to do so, produce a certificate
showing that the liquor in question was duly examined.
9.41 The licensee within one week of
their being made, but not later, may call in question, by an objection in
writing presented to the AETO any entries in those of the AETO’s registers
which are open to his Inspection. Any dispute regarding such entries which
cannot be settled by discussion between the AETO and the licensee shall be
referred to the Collector. If no objection is raised the entries shall be
presumed to be correct.
THE UPKEEP OF BUILDINGS AND PLANT
9.42 All buildings
and plant used directly for the manufacture and storage of wash and spirit must
be situated in a distillery enclosure in which no business shall be carried on,
except that of the manufacture, storage and issue of spirit. The enclosure
shall be surrounded by a wall having one opening only and so built as to
prevent communication between the distillery enclosure and outside, except
through the opening provided.
9.43 The buildings and plant shall be
specified in the license and shall be properly maintained to the satisfaction
of the Collector particular attention shall be given to their cleanliness.
9.44 The licensee
shall provide for use in measuring spirit in the distillery, and at the time of
issue such measures, gauging machines, weighting machines and other appliances,
as the Excise Commissioner may direct him to provide.
9.45 If the
building and plant (including the measures, etc referred to in the preceding
rule) are not properly maintained and the premises and plant are not kept
properly clean, the licensee may be required to stop all work in the distillery
within one week after receipt of notice to that effect from the Collector.
9.46 If any still
vat pipe or other part of the plant is at any time found to be defective or
leaking, and the Excise Commissioner or Collector order the discontinuance of
its use, it shall not be used again till it has been repaired to the Board of
Revenue’s or Collector satisfaction.
9.47 The licensee
shall not alter the building or plant specified in his license, without the
Director Excise and Taxation permission provided that any minor and urgent
alteration or repair may be made with the consent of the AETO, who shall
forthwith report to the Collector. Any important alteration sanctioned shall be
noted on the license.
9.48 All
processes for the manufacture, issue and sale of foreign liquor must be
conducted within the distillery enclosure.
STILLS AND OTHER PLANT PIPES
9.49 The
distillery and its apparatus shall be so arranged that from the time when the
fermented wash is passed into a still to the time when the spirit is issued
from the store vats, the distillate shall be contained in closed receptacles
and be conveyed to stills, receivers and other receptacles only through closed
pipes preferably by force of gravitation, but when this cannot be arranged, by
pumping. Water required for the distillery working shall be carried off only
through closed pipes, wash shall be conveyed from the fermentation vats to
stills and spent wash and spent lees shall be carried off in closed pipes or
covered drains.
9.50 The ends of
still worms and all pipes which carry spirit or serve spirit receptacles shall
be firmly fixed into the receptacles they serve.
9.51 If a spirit
pipe is required to charge or discharge one or other of a series of
receptacles, the pipe shall be connected with each of the receptacles, by half
unions of the same pattern fixed in the receptacles the other half of the union
common to all, being fixed to the connecting pipe.
9.52 All the
joints in spirit pipes must either be riveted or be joined with bolts. In the
later case, the flanges bolted together must have, in addition to the bolts at
least two rivets made of a composition of lead and tin, and sealed with a
revenue seal, or, in the case of certain joints when this is specially
permitted by the Excise Commissioner the flanges may be pierced by a bolt
carrying a revenue lock, inserted through a hole, at one end of the bolt.
Alternatively the flanges may be drilled with a hole 1/8th of an inch in diameter
through which a wire should be twisted together and sealed with a revenue seal.
9.53 The licensee shall be responsible for
preventing any leakage from pipes.
9.54 Pipes
intended for the conveyance of wash and spirit must be so fixed that they can
be examined throughout their entire length.
9.55 All pipes
and covered drains shall be coloured with a colour indicating the purposes for
which they are used as follow:-
If intended
for the conveyance of wash, green; if for the conveyance of spirit, red; if for
the conveyance of water or steam, white; if for the conveyance of spent wash
yellow if for the conveyance of gas or electric wires used for the purposes of
illumination or power, black if for the conveyance of molasses, blue.
LOCKS
9.56 The charging
and discharging pipes of potstills, all spirit safes and all mandoors, clocks or other openings in stills, spirit
vats, spirit receivers spirit chargers and other receptacles for spirit, and in
spirit pipes with branches, the point where each branch joins the pipes and the
doors of all buildings and rooms used for the storage of spirit shall be so
fitted as to enable them to be closed with two locks, the keys of which are not
interchangeable, and of which one lock shall be a revenue lock, in charge of
the AETO, and the other a distillery lock in charge of the licensee.
9.57 Revenue
locks supplied by the Excise Commissioner will invariably be put on whenever
necessary under these rules, but the licensee may dispense with his own locks,
except in the case of such as must be affixed to all receptacles or rooms used
for the storage of spirit.
9.58 Locks shall
be so arranged as to render it impossible to use any pipe or part of a pipe
unless the locks are either removed or else closed only with working
fastenings, or to extract any of the contents of any building, pipe receiver or
other receptacle concerned, without opening both the locks which control such
building, pipe or receptacle.
9.59 Lock
fastenings must be constructed as much as possible in one piece. When hinges on
them are necessary, the hinges must be formed by welded joints and not by
riveted pins. If a part of any fastening is attached to a door or a receptacle,
it must be by rivets and not by screws. The fastenings for locks must be fitted
so closely as not to admit of any cock being partially turned or opened or the
plug or key lifted up or taken out after the fastening is applied. Chain
fastenings must not be used, except in cases where it would be impracticable to
apply any other description of fastening.
9.60 When it is
necessary for the licensee’s operations that cocks upon closed pipes be left
open when the AETO is not present, working fastenings must be provided. Such
fastenings must be so constructed that the revenue lock shall not interfere
with the free use of the cock and so fitted that no abstraction of spirit is
possible.
GENERAL RULES AS TO ECEPTACLES FOR WASH, BUB SPIRIT AND DENATURED SPIRIT
9.61 Except for
the bona fide purposes mentioned below the licensee shall not introduce or
permit the introducing of bottles or other versels having a capacity of less
than four gallons each, into the distillery enclosure.
EXCEPTIONS
(i)
Bottles required for bottling country spirit or
Pakistan made foreign spirit under rule 9.93.
(ii)
Bottles or other vessels, in such number as may be
determined by the Board of Revenue containing essences, colours and the like
needed for the licensee’s legitimate operations but they should be stored in
the colouring and compounding material room referred to in rule 9.92.
(iii)
Bottles or other veseels intended for use as containers
of rectified or denatured spirit, to be supplied to Civil Surgeons or to
scientific institutions approved by the Board of Revenue and bottles approved
for bottling of rectified spirit under rule 9.93A of these rules.
(iv)
Bottles or other vessels for removal of products by the
distiller for purposes enumerated in rule 9.40, 9.40-A and 9.115 (g) of these
rules.
9.62
Vats shall ordinarily be used for the storage of
spirit, but a limited number of caskes or drums may, subject to the provisions
of rule 9.64 below be kept in the store room for the storage of special kinds
of spirit, such as whisky and for the use in collecting quantities withdrawn
from store vats in slight excess of requirements and the like, and a limited
number not exceeding 30 of caskes or drums filled according to rule 9.10 6 of
these rules for issue may be kept temporarily in the store room for issue to
purchasers.
9.63
The vessels used as receptacles may be of any
material; they shall be of regular shape large covered vessels shall be fitted
with manholes of a size approved by the Board of Revenue and every vessel shall
be provided with proper approved arrangements for gauging with rods and with
tables showing the number of gallons contained in them when filled to every tenth
of an inch by either the wet or the dry method of gauging according as the
Board of Revenue decides to apply one or the other method to such vessel. When
the wet method of gauging if applied to any vessel a permanent dipping rod of a
pattern approved by the Board of Revenue shall be fixed in a manner approved by
him to that part of the vessel where there is the greatest depth of liquid in
it.
9.64
Each vessel shall have legibly painted on it in
English its number, its capacity and the use to which it is applied and its
details shall be properly registered by Inspector.
9.65
Except with the special sanction of the Board of
Revenue in the case of a receptacle, sunk under the ground level each vessel
shall be fixed so as to permit of examination all around it shall slope
slightly down to its cock and its cock shall be so fitted that the vessel can
drain entirely through the cock without being moved.
9.66
No receptacle of which the contents are estimated
by a guage, rod, shall be brought originally into use till it has been gauged
and passed by the AETO and a table book has been prepared fot it, and, if any
gauged receptacle is repaired or moved, it may not be brought again into use
till its has been reguaged and passed by the AETO and revised table book has
been prepared.
FERMENTATION VATS
9.67 Fermentation vats shall be placed in a
room or building specially set apart for them alone.
9.68 The licensee
shall provide vats for the fermentation of wash having a capacity sufficient
for the continuous working of all the stills in the distillery, up to the
maximum of their capacity as recorded in the license upon the calculation that
it required 48 hours to ferment wash.
9.69 No wash shall be used except such as
has been prepared within the distillery, nor shall any wash be removed from the
distillery;
Provided that if so desired the licensee may be allowed to
remove samples of wash from each vat in quantity not exceeding half a gallon
per vat for use in the distillery laboratory;
Provided further that in the case of the preparation of wash
for the manufacture of malt whisky, the said wash may be prepared in the
Brewery and then pumped into a distillery for purposes of distillation.
9.70 The licensee
shall enter in the register prescribed for the purpose the exact quantity of
the gur, molasses, mahua or other substance used, and shall give the AETO an
opportunity of verifying this quantity whenever he may deem it desirable to do
so.
9.71 (a) If wash
is prepared from a malt base, it must be collected in the fermenting vat and be
ready for gauging and proving within six hours, after it has begun to run into
the vat.
(b)
In the case of wash prepared from gur or liquid
molasses, the AETO shall take the readings, as regards quantity and specific
gravity, as soon as complete solution has been attained. The solution may be
effected in the fermentation vat or in a dissolving vat separate from the
fermentation vat.
(c)
In certain distilleries, gur or molasses wash, prepared
in a dissolving vat, is run into a fermentation vat after the necessary
quantity of bub has already been introduced into the fermentation vat. In such
cases, the specific gravity of the wash in the dissolving vat, immediately
before transference to the fermentation vat should be treated as the initial
specific gravity of the wash. Where the
contents of two or more dissolving vats are transferred to the fermentation
vat, the initial specific gravity of the wash. Where the contents of two or
gravities of the valts in the several dissolving vats used, calculated where
necessary according to example II one page 124 of the Technical Excise Manual.
It would be an advantage to maintain a fixed specific gravity in the dissolving
vats.
(d)
If mahua is used, the initial quantity and specific
gravity of the wash shall be ascertained in such manner as the Excise
Commissioner may specially prescribe.]
9.72 (i) No
substance of any kind shall be added to the wash after it has been gauged and
proved, except water or chemicals or bub added under the procedure set forth in
the next succeeding clause, provided (i) that due notice of such addition is
given by the licensee to the AETO; (2) that
the requisite entries regarding it are made by the licensee in the
prescribed register; and (3) that no addition of any kind is made to wash more
than 24 hours after it was first gauged and proved. After the lapse of this
period of 24 hours, the wash shall remain undisturbed in the fermentation vat
until fermentation is completed and the wash is removed to the still.
(ii) In some
distilleries wash is prepared in a dissolving vat or vats separate from the
fermentation vats and is (a) gradually added to bub already collected in the
fermentation vat or (b) collected simultaneously, with bub running into the
fermentation vat. In the case of such distilleries, no substance of any kind
shall be added to the mixture of the bub and wash in the fermentation vat.
Water and chemicals may however, be added to the wash in the dissolving vat or
vats, before it has been gauged and approved. The initial quantity and specific
gravity of the mixture of bub and wash in such cases should be calculated from
the initial quantities and specific gravities of wash and bub ascertained
immediately before they are run into the fermentation vat.
9.73 (a) The
preparation of bub shall be conducted in a special bub vat or vats set apart
only for such preparation and the registration of the materials used and of
solution and other matters connected with it, shall be carried out in the
register specially prescribed for the purpose. The bub vats used may be smaller
than the ordinary fermenting vats if desired, and there may be connected with
it an auxiliary vessel for dissolving the material used for setting up the bub,
but fermentation must not be allowed to proceed to a close in this vessel.
Ordinarily the whole of the bub must be conveyed into the fermentation vat or
vats to which it is to be added within 24 hours of first beginning to make, or
dissolve or set it up.
(b)
With the special permission of he Excise Commissioner
any licensee who is able to declare the alcoholic percentage and the original
specific gravity of a bub may keep such bub for more than 24 hours after the
time when its making solution or setting up commences, and he may be permitted
to make such a bub for more than 24 hours after the time when its making
solution or setting up commences, and he may be permitted to make such a bub
and keep it going continuously by adding to it fresh safcharine substance and
water from time to time. In such a case he must, at the time of original book
adding any of such continuously maintained bub, to the contents of any
fermentation vat containing wash, record the quantity in bulk gallons, and the
original special gravity of the addition. The AETO shall enter a copy of these
particulars in his registers and make necessary alterations in the record of
the wash to which it is added.
(c)
The licensee shall give notice to the AETO, with
details of the registered numbers of the vessels concerned, before any
conveyance of bub from the vat in which it is prepared, to the main wash, or to
a fermentation vat.
9.74
As soon as wash is fully attenuated and ready for
distillation, the licensee shall inform the, AETO, and the AETO shall again by
guauging and the use of the Saccharometer, ascertain the quantity and specific
gravity of the attenuated wash and record these in his prescribed register. The
licensee shall record the final quantity and specific gravity in the register
prescribed for maintenance by him.
9.75
The licence shall not draw off or use the
attenuated wash until it has been gauged and proved by the AETO, and when he
does draw it off, the AETO shall enter in the prescribed register particulars
regarding the quantity drawn off and the still into which it is drawn off.
STILLS
9.76 Stills may
be of any form or construction the licensee may think proper and for which he
has a license, but the still power of the distillery shall not be increased
without the special sanction of the Excise Commissioner.
9.77 The Director
Excise and Taxation may authorize the replacement of any still by another of
equivalent distilling capacity, or the reuse of any still which has been
dismantled and thrown out of use without its place being taken by another
still.
9.78 There shall
be no openings into any still, except those in connection with the charging and
discharging pipes, pipes for the conveyance of vapours or fluids from one part
of the still to another condensers, mandoors an air cocks or valves upon the
breast or head. The external orifice of an air valve must be so constructed and
covered by a perforated metal plate as to make it impracticable by means of it
either to introduce wash or to abstract spirit or to convey away spirit vapour
for condensation elsewhere.
9.79 When wash is
being distilled in a pot still and in all distillations by a continuous still
the still need not be secured by the AETO with a revenue lock.
9.80 When a pot still is being used for
the distillation of unfinished spirit, the mandoor and the charging and
discharging pipes shall be secured by the AETO with closed fastening and a pot
still used for the redistillation shall be charged and discharged only after
notice has been given to the AETO and under his supervision.
SAFES
9.81 A safe
furnished with a hydrometer or specific gravity beeds, capable of showing the
strength of the distillate, shall be provided between every still and its
receiver or receivers. There may be separate safes between each still and its
receiver or receivers, or a central safe which controls the worm ends
communicating between a number of stills and their receivers.
RECEIVERS AND CHARGES
9.82 Two or more
receivers may be fitted to the same still in order to enable the distillate to
be collected in separate portions and one receiver may work, in connection with
more than one still. There should be a separate receiver for feints.
9.83 The receiver
or receivers attached to each still or set of stills shall be of a capacity
enabling them to contain all the distillate which can be produced by the still
or set of stills in 36 hours full working.
9.84 The spirit
whether finished or unfinished produced by any one distillation, shall be run
into an empty receiver or receivers, and such spirit shall be gauged and proved
by the AETO in the presence of the licensee or a responsible representative
deputed by him for this purpose, in the receiver or receivers of the still or
set of stills in which it is produced, before it is passed out of such receiver
or receivers or mixed with spirit produced by any other distillation.
9.85 The
admixture of sugar or other foreign substance in the spirit after it has been
drawn from the still and before it is tested is prohibited.
9.86 The AETO
shall arrange ordinarily to discharge into a still or charger, as desired by
the licensee directly after each distillation, all unfinished spirit run into
the receiver or receivers connected with such distillation, and to pass into
the store vats each evening all spirits finished during the day and each
morning all spirits finished during the night, and he shall, by the use of the
gauge and hydrometer, verify and record in the prescribed registers the
quantity and the strength of all spirit so discharged or passed in.]
STORES VATS
9.87 Store vats
shall be kept in a room or building set apart entirely for them and provided
with only one door. This room or building will be designated the store room.
9.88 The licensee
shall provide store vats, having an aggregate capacity equal at least to half
of the demand of the month in which most spirit is issued during the year. If
the existing capacity at any time appears from the average of the issues,
recorded during the previous three years, to be materially deficient, the
licensee shall, if required by the Director Excise and Taxation make the
necessary increase to it.
9.89 A store vat or vats may be separately
set apart and used for the storage of each of the
following kinds of spirit viz:-
(1)
Plain spirit.
(2)
Spiced spirit including special spiced and matured
spirit.
(3)
Pakistan Made foreign spirit.
(4)
Denatured spirit.
Provided that, excepting denatured spirit any vessel set
apart and used for the
storage of any one of the above kinds of spirits shall not
be used for the storage of any other kind of spirit, unless the vessel is
properly cleaned and filled with water for at least 24 hours so that no smell,
taste or colour of a previous sprit is imparted to a fresh spirit.
Any vessel or vessels set apart for the storage of
denatured spirit shall be in a
separate room or building set apart solely for such spirit.
That room or building shall be called the denaturing room.
9.90 With the previous sanction of the
Excise Commissioner country spirit or Pakistan made foreign spirit intended to
undergo the process of maturing may be stored, without prepayment of duty in an
unlimited number of cases in a room within the distillery enclosure specially
set apart and used only for this purpose and secured under the double lock of
the AETO and the licensee. The spirit for maturation may, with the special
permission of the Excise Commissioner be kept in wood vats and in spirit store
room which shall for the purposes of this rule be deemed to be a matured spirit
warehouse. The room will be designated the matured spirit warehouse Deposits
in, and withdrawals from the warehouse will be governed by the following
regulations:-
(1)
An application for the removal of country spirit or
Pakistan made foreign spirit from the store room to the matured sprit warehouse
must be made in writing to the AETO. The application, on presentation must
specify the serial number of each cask, and before removal takes place must be
completed by specifying for each cask its full capacity and the quantity and
strength of the spirit it contains.
(2)
Removals may be made at any strength not below the
strength prescribed for the issue of spirit.
(3)
No. cask of less than eight gallons capacity shall be
removed for deposit in the matured spirit warehouse.
(4)
In preparation for removals, the tare or weight empty,
of each cask must first be ascertained the cask thereafter filled to the
bunghole with the spirit intended for removal and the capacity determined in
the manner prescribed by the Excise Commissioner No objection need be raised if
it is desired to draw off any quantity by imperial measures from the full cask
before the removal is made. In that case, the quantity remaining in the cask,
i.e. ullage quantity will be reckoned by deducting the measured quantity from
the ascertained full capacity.
(5)
All Particulars of gauge and proof must be recorded at
the time of removal in the appropriate columns of the warehouse register,
instead of on the pass, as in the case of ordinary issues. The quantity in
London Proof gallons will be shown as transferred to the warehouse in the
appropriate column of the issue register but it is important that the removal
should not be classed with the issue.
(6)
Upon the outside of both of the heads of every cask
removed from the store room for deposit in the matured spirit warehouse must be
legibly printed with oil column the progressive number of the cask beginning
with number one on the first of January in each year, also the colander year in
which the deposit is made and the full capacity to the nearest tenth of the
gallon.
(7)
No pass will be necessary to cover transport from the
spirit store room to the matured spirit warehouse.
(8)
Immediately preparation for removal has been completed
the AETO must see the cask or casks safely deposited in the warehouse.
(9)
Each cask deposited in the warehouse must be closed
with a bung of hard wood, fitted flush with the cutside of bung stave. The
licensee may in his discretion, insert a spiget in to the hard wood bung, to
serve as a safety valve.
(10)
Casks must be so arranged in the warehouse as to allow
easy access to them in order that a correct account of their contents may be
taken at any time and leakages may be readily discovered.
(11)
It will be unnecessary to take monthly account of the
spirit in stock in the matured spirit warehouse as in the case of spirit in the
store room. The stock of spirit in the warehouse shall invariably be the total
quantity in London Proof gallons as shown in the warehouse register. The
collector or the Excise and Taxation Officer may occasionally check the
quantity of the spirit in a few of the casks in the warehouse and record the
result briefly in the warehouse register. Where they find that the deficiency is
in excess of the scale prescribed by the Excise Commissioner, they shall
inquire into the cause and satisfy themselves that no illicit abstraction from
the casks has occurred. The Inspector shall be responsible that the casks,
while in the warehouse, are not tempered with unless in his presence and in the
presence of licensee or his manager, for the sake of repairs or for the
examination of the spirit by the Collector or Excise and Taxation Officer, and
unless such tempering with is necessary. The AETO should make, each month, a
careful inspection of the apparent condition of each cask lying in the matured
spirit warehouse and arrange for the immediate transference of the contents of
a cask found leaking. The result of each inspection should briefly recorded in
the warehouse register and a note, that the usual inspection has been made,
should also be entered in the AETO’s diary in form D-9.
(12)
Reduction of contents of a cask is not permitted in the
warehouse. Removals from the warehouse will be made to the store room, where
reduction can be effected before the spirit is finally issued from the
distillery. No objection need be raised, however to the introduction of a new
cask, whose full capacity has been first ascertained, for reception of the
contents of a defective cask in the warehouse. When this is necessary, the AETO
will have the spirit transferred to the new cask, which must be marked and
numbered similarly to the old one, make a note of the transfer in the warehouse
register.
(13)
No removal of the contents of a cask is permitted from
the warehouse to the store room.
(14)
Removal will be made from the warehouse to the store
room on the written application of the licensee specifying the progressive
number of the cask, the year when warehoused and (on its removal) the ullage
quantity and strength.
(15)
On receipt of the licensee’s application the AETO will,
after taking account of the spirit in the cask by means of the bung rod in the
manner prescribed by the Excise Commissioner see the casks removed to the store
room from which the issues of matured spirit will be made under the ordinary
rules and procedure. The actual quantity of the spirit in London Proof gallons
removed from the warehouse to the store room will be recorded in the warehouse
register as passing into the stock of the latter.
(16)
The deficiency allowable during the period of storage
in the warehouse is calculated according to the scale prescribed by the Excise
Commissioner. In the event of deficiency being in excess of the prescribed
scale, the Inspector will make a brief report in the warehouse register on the
condition of the cask on delivery actually i.e “no apparent cause” in cases
where the cask is in an apparently sound condition, and a few brief remarks
where such causes as leaks, defective staves, broken hoops, dorous wood etc,
might account for the excess.
The Excise and Taxation Officer at his inspection will
enquire into the reasons given
for the excess, and if he is satisfied will initial he
AETO’s entry in the warehouse register. If he is not satisfied that the excess
is due to natural or accidental cause, he will submit a report, recording his
reasons at full length, to the Collector so that action for recovery of duty on
the excess may be taken under rule 9.102 if necessary.
MANUFACTURE, STORING AND PASSING OUT OF SPIRIT
9.91 Blending or
reduction of plain spirit is permitted in the store vats, provided the blending
and reduction is done in the presence of the AETO and under his supervision.
Any other blending or reduction as is desired may be done at the time of issue
in the special issue room mentioned in rule 9.103 below. Water used for
reduction must be pure, and the licensee must comply with the directions of the
Collector regarding the water supply.
9.92 The colouring and / or compounding of
spirit with materials not specifically prohibited by the Excise Commissioner is
permitted.
(a)
in the store vats.
(b)
In the special issue room (rule 9.103) at the time of
issue; and
(c)
In bottling vats or other vessels in which spirit is
stored before transference to the bottling room.
Provided this is done in the
presence of the AETO and under his supervision.
All colouring and compounding
materials brought into the excise enclosure shall be entered by the AETO in the
register n form D-16 and is kept thereafter in the colouring and compounding
materials room. Their quality and character shall be subject to check as
occasion may require.
9.93 Subject to
the approval of the Excise Commissoner, operations connected with the filling
of bottles with country spirit and Pakistan made foreign spirit for issue shall
be conducted in bond under the supervision of the Distillery AETO, in separate
rooms called bottling rooms for country spirit and Pakistan made foreign spirit
respectively, set apart for the purpose, within the distillery enclosure near
the spirit store, (For the duration of the present war, the bottling of
Pakistan made Foreign Spirit may be carried on in the bottling room for country
spirit, provided that a separate charge and bottling machine shall be provided
for the bottling of Pak-Indian indeed Foreign Spirit in such room). In these
rooms the licensee may set up such apparatus for filtering, bottling and
processes connected therewith as may be needed. Bottled spirit shall be stored
in separate rooms called the bottled spirit store for country spirit and
Pakistan made Foreign Spirit, respectively set apart for the purpose within the
distillery enclosure near the bottling room. The bottling rooms and the bottled
spirit store rooms shall be secured in such manner as the Excise Commissioner
may approve. In the bottling rooms bottling vats may be erected and spirit
stored therein. The following rules shall be observed for the conduct of
bottling operations:-
(a)
Country spirit and Pakistan made foreign spirit shall
be bottled at the strength from time to time prescribed by the Excise
Commissioner.
(b)
Bottling shall be done during the ordinary working
hours of the distillery. If the licensee has reduced the strength of the spirit
by blending or otherwise, he shall not bottle the spirit until 12 hours after
operations are complete, unless arrangements approved by the Excise
Commissioner have been made to cool the spirit to a normal issue temperature
thereby preventing shrinkage in bottles after issue.
(c)
No bottles shall be filled with spirit except in the
joint presence of the AETO and a representative of the licensee.
(d)
Spirit required for bottling shall be measured out and
brought into the bottling room by a permanently fixed pipe (bearing, within the
spirit store, a cock and fastening for an Excise Book) or such other means as
may be approved by the Excise Commissioner.
(e)
Bottles and flasks of the following sizes only shall be
used:(i) Quarter bottles of the
capacity of 6 2/3 ounces.
(ii)
Reputed pint bottles of the capacity of 13 1/3 ounces.
(i) Reputed quart bottle of the capacity of 26 2/3 ounces.
The licensee shall not use for
bottling spirit any bottles or flasks bearing the name or trade mark of any
other bottler or any other distillery. The Excise Commissioner may accord
permission to a licensee for a period not exceeding six months to use such
bottles or flasks of another distillery with the conscent of that distillery
provided that variations in the size of bottles and flasks to the following
extent shall be permissible for the purposes of this subrule:-
Capacity of bottles & flasks
Variations permitted.
6 2/3 ounces 1/8 ounces
13 1/3 ounces ¼
26 2/3 ounces 3/8 ounces
(f)
The bottles and the flasks mentioned in sub-clause (e)
above shall be of standard pattern.
For the
bottling of country spirit they shall bear the following specifications moulded
or sand blasted on the glass:(i) the words Punjab Excise
(ii)
the figures and the words 26 2/3 ounces, 13 1/3 ounces
or 6 2/3 ounces in the case of reputed quarts, pints and quarter bottles respectively.
(iii)
The name or mark of manufacturer of the bottles, and
(iv)
A line across the neck upto which the bottles shall be
filled in order to contain the proper quantity.
For the bottling of Pakistan
made foreign spirit they shall either bear the same specifications moulded on
the glass as prescribed for the country spirit or shall have a monogram moulded
or sand blasted on them consisting of the letter “P.E” and the figures and
letter 26 2/3 ounces 13 1/3 Ounces or 6 2/3 ounces.
(ff)
Notwithstanding the provisions contained in sub-rule (f) above, the Excise
Commissioner in case of emergency, may permit the use of non-standard pattern
bottles, without the name or mark of the manufacturer of the bottles or a line
across the neck and also to sand blast letters P.E instead of the words Punjab
Excise on pints and nips to be used for the bottling of country spirit. Such
non-standard bottles shall be of the capacity approved by the Excise
Commissioner.
(g)
All bottles mentioned in sub rule (e) above, shall be
securely sealed with a lead capsule cemented with improved quality of
cementation to the bottles in such a way as to make it impossible to remove the
capsule without its being torn. The capsules shall bear (i) the name of the
distillery and (ii) the kind of liquor bottled at the top and shall be twisted
round the neck of the bottle by means of a machine.
(h)
The licensee shall use the following kinds of capsules
for the different kinds of
liquor:-
(i)
For plain spirit Plain capsules
(ii)
For spiced spirit Brilliant capsules of different
colours (ii) For special spiced
spirit Wax finished capsules.
(iii)
For foreign made Ordinary pilfer proof capsules.
The word capsule appearing in
this clause includes aluminum capsules of good quality. All the capsules shall
bear in black letters the information set forth in clause (g) above. The
degrees of obscuration shall be shown on the capsules or otherwise on the label
mentioned in sub-rule (1) if the obscuration exceeds two degrees. With the
previous sanction of the Excise Commissioner only to be given in exceptional
circumstances of which the Excise Commissioner shall be the sole judge, a
licensee may use plain capsules on bottles containing spiced spirit or coloured
capsules on bottles containing plain spirit, or the capsules of another
distillery with the consent of that distillery. Provided that the Excise
Commissioner may in case of emergency permit the use of plain capsules, without
the superscription of emergency permit the use of plain capsules, without the
superscription required by clause (g) (i) and (ii) above. Provided further that
with the permission of the Excise Commissioner the licensee may emboss the
required superscription on the capsules in self colour instead of in black
letters as prescribed above.
(i)
Unless otherwise specially permitted by the Excise
Commissioner plain country spirit shall be bottled in dark glass bottles or
flasks and spiced spirit, including special spirit, including special spiced
spirit whether coloured or uncloured in clear glass bottles or flasks.
(j)
The licensee shall not use taper corks for bottling.
The licensee shall soak the corks in clean water for 24 hours before corking
the bottles.
Provided that with the
permission of the Excise Commissioner which will be granted in exceptional
cases, the licensee may use crown corks in lieu of ordinary corks on bottles
used for bottling of plain country spirit. Crown Corks will not, however,
replace the use of capsules required under sub rule (h) above.
(k)
The licensee shall label each bottle after bottling,
with a label showing the following particulars:-
(a)
the name of the distillery.
(b)
The district in which it is situated.
(c)
The kind of liquor bottled.
(d)
The strength of the liquor in degrees of proof.
(e)
The degree of obscuration and
(f)
In case of country spirit the words “Desi Sharab” in Persion
characters.
Provided that the strength of
the liquor and degrees of obscuration need not be shown on labels to be used on
bottles containing Pakistan made foreign spirit.
(l)
Before brining any label into use the licensee shall
submit exact copies thereof in quadruplicate, to the Collector who shall
forward them to the Commissioner for his approval. The commissioner if he
approves of the label, shall number it and affix his official seal. One copy
will be retained in the Commissioner’s Office for record. The remaining two
copies will be return to the Collector who will send one copy each to the
distillery AETO and the licensee for information and record. The licensee shall comply with such
instructions as the Commissioner may issue regarding any label. If the licensee desires to affix any more
labels to the bottles, he shall submit specimens for approval in the manner
prescribed above. Secondary labels need not have printed on them all the
details required for the main label. In particular the licensee shall carry out
the following directions:-
(i)
All labels required to be used on the bottles of spiced
spirit shall bear the word “masaladar” in Urdu and English character and the
words “spiced spirit” in English characters.
(ii)
Labels bearing the words “Superior” or “Special” shall
only be used on the bottles of special spiced spirit. Labels bearing the words
“Old” or “Matured” shall only be affixed to bottles containing spiced spirit
that has been kept in the matured spirit warehouse for more than two years in bond
from the date of distillation.
(iv) The words
“Rum” or “White Rum” shall not be used on labels to be affixed to bottles
containing malt whisky only, as defined in these rules.
(iv)
The words “Malt Whisky” shall only be used on labels to
be affixed to the bottles containing malt whisky only, as defined in these
rules.
(v)
The labels on the blended product of malt whisky made
in the Punjab distilleries and of imported scotch whisky shall described it as
“Pakistan Malt and Scotch Whisky Blend”.
(vi)
The words “Matured Whisky” shall be used only on
bottles containing matured whisky, as defined in these rules.
(m)
Labels must be so affixed as to be easily
distinguishable. No label shall be pasted over the words Punjab Excise and the
figurers and words 26 2/3 ounces 13 1/3 ounces, moulded or sand blasted on the
bottles. The approval of the label by the Excise Commissioner implies that
there is no objection to the label from the stand point of excise
Administration. It does not grant a copyright.
(n)
An account of spirit received and used for bottling
shall be maintained in form D.13B.
(o)
Except with the special permission of the Excise
Commissioner the Punjab Excise bottles shall not be used for bottling any
country or Pakistan made foreign spirit which is intended for export to another
province or to a Indian State. Such spirit shall be bottled either in plain
bottles or in bottles bearing such marks and indications not being those
approved for the Punjab as may be required by the State which conform to the
Punjab Regulations regarding the saleable strength of spirit and the size of
bottles, the spirit bottled for export may be issued at such strength and in
bottles of such size as may be required by the regulations of the State or
Province concerned, provided that the strength of spirit thus issued, shall not
be lower than that prescribed for the Punjab. Such bottling shall take place on
days other than those on which bottling for the Punjab and Punjab States takes
place, or if done on the same day, it must be done in a separate room. Such
spirit shall also be stored separate from that meant for the Punjab or Punjab
States. The Capsules and labels to be used on spirit bottled for export to
other provinces or states, other than the Punjab States shall be of such design
and bear such words as may be required by the excise authorities of the
destination to which the liquor is to be consigned. The label shall clearly
state the name of the province or state to which the spirit is to be exported.
If the labels used resemble those approved for use in the Punjab, they shall be
over printed with the words “For sale in the Province/or State only” The type
to be used for such overprinting shall not be smaller than two line pica.
9.93-A Rectified spirit may be bottled
with the previous approval of the Excise
Commissioner subject to the following conditions.
(a)
Operations connected with the filling of bottles with
rectified spirit shall be conducted in a separate enclosure called “The
Bottling Room for Rectified Spirit”.
(b)
Bottling shall be done during ordinary working hours of
the distillery in the joint presence of the Inspector and a representative of
the licensee.
(c)
Spirit required for bottling shall be measured before
bottling.
(d)
The licensee shall use bottles, corks, labels and
capsules as have been approved by the Excise Commissioner.]
(e)
Each bottle shall bear a label showing the following
particulars in blue:(i) Name of
distillery and the name of the district in which it is licensed.
(ii) quantity of rectified spirit contained in each bottle.
(v) strength of spirit in degrees of proof.
(iv)
the words “Rectified” spirit in English, English and
Urdu Characters, and
(v)
the words “Not intended for internal consumption except
under medical advice”.
(f) Bottles and
labels used for bottling rectified spirit shall not resemble in colour or
pattern, those permitted for the use of bottling country spirit or Pakistan
made foreign spirit.
9.94 Manufacture of ginger wine, milk punch
and medicated wine.
(i)
Ginger wine, milk punch and medicated wines shall be
manufactured and bottled in the prescience of the AETO.
(ii)
The spirit whether plain or sophisticated, required for
the manufacture of these wines, shall be measured out from the bonded store
room of the distillery.
(iii)
The duty on these beverage shall be charged in the same
way as in the case of other spirit stored in the distillery. Pending the issue
from the distillery, the bottled stock thereof shall remain in bond under lock
and key.
DENATURATION OF SPIRIT
9.95 For the
purpose of rendering spirit effectually and permanently unfit for human
consumption no substance other than light caoutchoucine and mineral pyridine
bases shall be used. They shall be mixed with the spirit to be so rendered
unfit for human consumption in the proportion of one half percent by volume of
caoutchoucine and one half percent of mineral pyridine bases to the whole
volume of the spirit which shall be of not less strength that fifty degrees
over proof.
Provided that the previous sanction of the Excise
Commissioner is obtained in each case, the use of wood naptha as a sole
denaturant is also permitted for denatured spirit to be supplied to the
Pakistan Medicinal Store Depots. One part by volume of crude wood naptha of the
specifications mentioned in rule 9.126 of these rules and nineteen parts of
spirit of a strength of not less than 50 degree over proof shall be mixed to
prepare such denatured spirit.
Provided further that if the spirit to be removed is
required for use in particular process, the Excise Commissioner on special
application being made to him may authorize special methods of denaturation.
9.96 The
specifications of light caoutchoucine and mineral pyridine bases shall be those
from time to time approved by the Excise Commissioner.
9.96-A Specially denatured spirit of the strength of not less than
60 degrees over proof may be issued to soap manufactures provided that it is
denatured with the following denaturants:(a) half percent caustic soda.
(b)
Three percent castor oil soap;
(c)
One percent of the volume of wood naptha or methyl
alcohol.
The specifications of caustic soda and castor oil soap and
alcohol are given as follows:-
CAUSTIC SODA to be used should contain at least 90 percent
active Sodium Hydroxide and when dissolved in water should form a clear
solution.
CASTOL OIL SOAP. Should be made from pure filtered castor
oil with a filtered caustic soda lye made from 76 percent or less than 25
percent of water 5 gms of the soap shoul be able to dissolve into a clear
solution in 50 cc of hot distilled water. It should be absolutely free from any
fillers what so ever. A portion of the soap when placed on an un-glazed paper
should not show any stain. The insoluble free fatty acids obtained from the
soap should have an iodine value between 85 and 92 and acid value between 190
and 195, melting point between 10 and 13 degrees Centigrade and refractive
index 1.4525 to 1.4565 at 60C. The acids should be carried as follows:-
Dissolve the soap in hot distilled water and add a slight
excess of Hydrochloric acid. Heat the mixture on a water bath until the fatty acids form transparent layer at the
top. Separate the fatty acids by means of a separatory funnel and wash them
with hot water until the washed waters are neutral when they are treated with
Methyl Orange. Transfer the acids in a dry beaker and heat them at 100c in an oven
for about 1½ hour. The acids thus dried should be tasted for iodine value, acid
value, refractive index etc.
The alcohol
or rectified spirit used should be not more than 66 c or less than 60 c over
proof.
For denaturing 100 gallons of rectified spirit the process
recommended is as follows:-
Take the rectified spirits in the tank and add to it 30 lbs
of castor oil soap as specified above, little at a time and stir the mixture
continuously until it is completely dissolved. A slight turbidity may be overlooked
take 4 lbs of caustic soda and dissolve it in 2 gallons of water. After the
caustic soda has been completely dissolved allow the solution to cool and
settle. When the solution comes to the rooms temperature and the clear solution
to the soap alcohol mixture. Stir it well and allow the mixture to settle. The
clear denatured alcohol thus obtained is then ready for distribution. The
denatured alcohol should have the following properties:-
10 cc of denatured alcohol should require in less than 9.00
and more than 11.00 cc of 0.1 normal Sulphuric acid.
9.97 No
consignment of denaturing materials intended for use in rendering spirit
permanently and effectually unfit for human consumption, shall be brought into
a distillery otherwise than with the permission of, and in the presence of the
AETO.
9.98 The licensee
shall provide a special room for the storage of the denaturing agents and
vessels and receptacles used in the process of denturation, and the process
shall be carried out in this room only, and in the presence of the AETO. After
denaturation is competed, denatured spirit shall be immediately issued or
stored in the special room, which shall be secured by double locks, the keys of
which are not interchangeable. The key of one lock shall remain with the AETO
and the key of the other lock shall remain with the licensee.
9.99 For the
purpose of satisfying himself that the denaturing materials stored in any
licensed distillery are efficacious for the purpose of rendering spirit
effectually and permanently unfit for human consumption, the Collector shall,
from time to time, but not less than twice in each year, send a sample of every
separately stored quantity of such denaturing material to the Chemical Examiner
to Government Punjab, for the purpose of being tested and its quality and
efficacy being reported upon.
No spirit stored within a licensed distillery shall be
denatured otherwise than with the permission of, and in the presence of, the
AETO.
9.100 For the
purpose of ascertaining that spirit has been effectively and permanently
rendered unfit for human consumption in the manner prescribed, the Collector in
whose jurisdiction the distillery is situated shall, not less than once in
every three months, and without previous notice to the licensee, cause to be taken
from stock a sample of such spirit, amounting to above six fluid ounces, and
shall send such sample to the Chemical Examiner to Government, Punjab, for
examination and report. A copy of the report of the Chemical Examiner shall be
submitted to the Excise Commissioner.
WASTAGE AND LOSS
9.101 Deleted,
vide notification No.301-68/368-Ex.III dated 17.2.1968.
9.101-A (1) The
Excise Commissioner prescribes that the scale of wastage of spirit shall be 2
percent for spirit store room, I percent for bottling operations and I percent
for bottled spirit store room in distillery.
(2)
Wastage shall be calculated for each month but charge
on accounts of duty
shall be made up at the end of the financial year, and the
distilleries will be allowed to set off the results of moths in which the
wastage of spirit was less than the prescribed standard against the results of
months when the wastage exceeded the standard.
(3)
Duty shall be charged, as on manufacture at the rate of
still head duty
applicable to the particular kind of spirit, subject to the
following exceptions:-
(a)
no duty on the excess wastage of denatured spirit shall
be charged, provided denatured spirit is stored separately within the
distillery enclosure as such and.
(b)
Duty, if any, on the excess wastage of matured spirit
shall be changed under rule 102 read-with sub-rule 16 of rule 90, an not under
rule 101-A.
(4) Deleted, vide notification No.714/Ex. dated 2.4.1954.
9.102 In case
extraordinary wastage of spirit occurs in a distillery owing to any cause, an
enquiry into the circumstances shall be made immediately under the orders of
the Collector or Excise Commissioner and if it is found that the wastage was
due to preventable causes, which the license should have foreseen or guarded
against, and that the spirit was required to meet a demand, made on the
distillery, the meeting of which was delayed by reason of the loss, the
licensee shell if directed to do so by the Excise Commissioner pay all or such
part, as seems reasonable of the duty that would have been recovered on the
wasted spirit, if it had been issued.
9.103 A special
issue room shall be provided by the licensee near the spirit warehouse for the
operations connected with the filling of vessels for issue and their issue form
the distillery.
9.104 No vessel
shall be filled with the spirit for issue, except in the joint presence of the
Inspector and of a representative of the licensee.
9.105 In the
process of filling vessels for issue spirit from different stores, vat may be
blended according to calculation, or water may be added for the purpose of
producing spirit of a strength required, but the AETO shall record the actual
quantity and the strength of the spirit actually drawn from each vat.
9.106 Spirit may
be measured into a vessel for issue by being passed directly from a store vat
into the issue vessel through a pipe or armoured hose attached to the cock of
the vat and discharging into a gauging machine placed in the issue room at a
convenient level, to discharge into vessels placed under it, provided that, when
this cannot be arranged, spirit may, with the Director Excise and Taxation’s
sanction be measured in a vessel for issue by means of gallon measures. Spirit
may be passed through a filter before it enters the gauging machine. Separate
vessels shall be used for measuring potable and unpotable spirit.
9.107 Before a
gauging machine is brought into use the AETO shall verify its correctness with
his standard measure and he shall with the measurers 7 verify it on the first
and 15th day
of each month.
9.108 The
licensee is responsible for securing the bungs or other openings of all casks
and vessels filled for issue and for preparing them, or, if they are packed,
preparing their packages, for sealing by the AETO in such a way that they
cannot be opened without damaging the seal.
9.108-A The AETO
shall weigh the empty casks and the casks filled with the spirit and record the
weight in the register in form D.22 if the check by weightment shows an excess
or deficiency of more than two pounds in 40 gallons, the liquor should be
re-measured. As issues are made by measurement and not by weight the result of
weightment should not be accepted as final without re-measurement.
9.109 In case the
licensee is required to issue spirit of specified strength, he shall, if the
Excise Commissioner so directs have a label of a special colour prescribed by
the Excise Commissioner for each such specified strength, at which spirit is
issued by him and shall put the appropriate label on each vessel and package
before presentation to the AETO for sealing.
9.110 The
licensee shall not decline sale or refuse supplies to any licensed vendor,
wholesale or retail, who has obtained a permit for the issue of spirit from his
distillery and tenders payment for such spirit at the rate the current. If more
than one licensed vendor be applying at one time for supplies, in case of
dispute who shall be supplied first the licensee shall supply them in order of
the dates of the applications received by the AETO, the decisions between the
applications bearing the same date, being made by the AETO by lot, provided
that not more than 500 gallons shall be supplied at one issue to a licensed
vendor who desires an issue of bottled spirit or in the case of bulk spirit who
desires his issues to be made in casks of capacity of at least 40/45 gallons
each supplied by himself or by the distillery on his behalf, and tendered at
the time to be filled, and that not more than 45 gallons shall be supplied at
one time to a licensed vendor tendering vessels of a smaller capacity. If any
customer cannot with due diligence, be supplied before a notified change of
price takes place, the licensee may demand payment from him at the changed
price in force when he is actually supplied.
GENERAL RULES REGARDING THE ISSUE OF SPIRIT
9.111 No bulk
spirit shall be issued in quantities of less than four gallons and no bottled
spirit shall be issued in quantities of less than two gallons except when
spirit is issued as a sample in accordance with rule 9.115(g) below. The removal of any spirit other than bottled
spirit shall not be permitted in vessels of less than four gallons capacity.
This
restriction does not apply to rectified spirit issued duty free to hospitals
and dispensaries in the Punjab or other provinces and Pakistan States, provided
that the aggregate quantity issued on any one indent is at least one bulk
gallon. Notwithstanding any thing contained in this rule, for the duration of
the present war, the minimum quantity which may be issued in bulk shall be two
gallons.
9.112 No spirit
shall be issued till its quantity and strength have been verified by the AETO
or in the case of spirit flavored and coloured to suit a special taste, under
the special arrangements made for verification of its strength. All spiced
spirit except aniseed spiced spirit which turns milky white on dilution, shall
be coloured before issued to licensees
in the Punjab.
9.113 The
licensee shall, if required to do so by the Excise Commissioner issue spirit
only in, specified strength either generally or for particular classes of
purchasers.
9.114 No spirit
shall be issued except under a distillery pass
9.114-A The AETO
shall issue on the same day spirits indented or indents received by him up to
12 noon. No spirit shall, however be issued outside the hours prescribed in
rule 9.28 above. Any indent, which cannot be complied with on the same day,
shall be complied on the next working day. Indents received after 12 noon
cannot ordinarily be expected to be complied with until the next working day.
9.115 (1) A
distillery pass for the removal of spirit fit for human consumption may be
granted in favour of any of the following persons only, namely:-
(a)
a person certified to be holding a license in the
Punjab or North West Frontier Province to sell such spirit by whole sale or
retail and, when the spirit is to be transported or exported beyond the limits
of the district in which the distillery is situated, holding a permit signed by
the Collector or other officer authorized in that behalf, of the district of
destination.
(b)
an officer of the Supply and Transport Corps or
commanding a regiment of the Pakistan army holding a permit signed by the
Collector of the district of destination, or presenting a requisition
countersigned by the Brigade Commander or corresponding superior officer, when
it is proposed to export spirit for the use of troops serving outside the
territorial limits of Pakistan;
(c)
a person holding a permit signed by the Collector of a
district in any other province of Pakistan for the export of such spirit from
the Punjab into that district.
(d)
A person holding a permit signed by an officer duly
authorized in that behalf for export of such spirit to a State.
(e)
A person holding a permit from the Collector of any
district in the Punjab or North west Frontier province to transport, export or
remove rectified spirit or wine to such district for chemical or medical
purposes; and
(f)
A provincial or Divisional Darbari authorized by the
Collector to remove specially prepared spirit.
(g)
The manager of a distillery in respect of spirit issued
is samples; provided that:
(i)
spirit issued as samples does not exceed five I.P
Gallons per month;
(ii)
Samples are issued in bottles of the sizes specified in
rule 9.93 above or in bottles of any size smaller than the quarter bottle; and
(h)
an officer of Government in respect of spirit removed
by him in his official capacity.
(2) A
distillery pass for the removal of denatured spirit may be granted in favour of
any of the following persons only, namely:-
(a)
a person certified to be holding a license in the
Punjab or North West Frontier Province to sell such spirit.
(b)
A person authored by the Collector of any district in
the Punjab or North West Frontier Province or Delhi Province to remove such
spirit for industrial use; and
(c)
A person holding a permit signed by an officer duly
authorized in that behalf for export of such spirit to Indian State.
9.115 When
the licensee desires to remove from bond any quantity of fusel oil, a sample
shall be forwarded to the Chemical Examiner for analysis; and if the result of
the analysis shows the percentage of alcohol to be less than 15 per cent proof
spirit the fusel oil shall be issued under a pass in form D 20 free of duty.
9.116 Subject
to the provisions of rule 9.110 the licensee may act as an agent in removing
spirit for any licensed vendor including any whole sale agency licensed in the
name of a distillery who to enable the licensee to obtain a distillery pass
furnish him with a certificate showing that he is a licensed vendor.
9.117 Every
application for a distillery pass for the removal of spirit shall be made in
writing to the Inspector and shall be accompanied by the certificate or a
permit required under the relevant subclause of rule 9.115 above, such
certificate or permit being either a general one for the purpose of removals to
be made from time to time or a special one for the purpose of a single removal.
9.118 If
the applicant tenders cash in payment of still head duty the AETO, shall, after
ascertaining that the licensees, price has been paid, fill up the challan, for
presentation with the cash, at the treasury or sub-treasury of the district in
which the distillery is situated. The applicant shall present the treasury
receipt in token of his having paid the duty and the AETO shall affix it to the
counterfoil of form D.20.
9.119 The
applicant for a distillery pass shall be responsible for the correct
calculation and full payment of the still head duty due upon the spirit to be
removed, but, if he is in doubt as to the amount of such still head duty, he
may prior to its payment in the treasury apply t o the AETO for and revision of
the calculation.
In calculation duty on bottled spirit 24 half pints 12 pints
or six quart bottles shall be reckoned as one gallon.
9.120 If,
in removing spirit from the distillery as an agent for a licensed vendor, the
licensee prefers not to pay duty at the time, he may remove the spirit subject
to the adjustment of such duty against an advance payment made by him in to the
Government treasury on account of the duty recoverable on such removable. Such
replanshied, it must be by a sum that will bring it up to at least Rs.2,000/-.
The Treasury Officer will keep the Inspector informed of all payments credited
to an advance, and the Inspector shall maintain a statement showing such
payments and the duty debit against them. He shall balance this statement on
every day on which the distillery is open for the issue of spirit, and on every
such day shall inform the licensee of the balance standing to his credit and he
shall permit the removal of spirit of which the duty is debitable against the
advance only so long as the balance is not exhausted.
9.121 In
addition to the methods described in rule 9.118 and 9.120 above, spirit may be
removed from a licensed distillery (a) free of duty in bond and (b) on the
execution of a bond in form D.19 for the payment of duty. Removals under (a)
require in each case the sanction of the Collector while payments of duty in
arrears under (b) can only be authorized by the Excise Commissioner.
9.122 If
the inspector is satisfied that the applicant is entitled under rule 9.115 and
9.117 above to remove spirit, and that the still head duty has been paid or
accounted for in one of the methods prescribed in rule 9.118, 9.120 and 9.121,
he shall issue the spirit. At the same time he shall make over a pass in the
form prescribed (form D.20) sending a duplicate to the AETO of the district of
destination.
PRICES
9.123 The
licensee shall maintain in the office of the Distillery AETO a statement of the
price current for plain spiced and special spiced country spirit, bulk as well
as bottled, and shall not alter such price current except after 24 hours notice
to the Collector. The price current statement and every notice of alter nation
of prices shall be conspicuously posted in the general office of the distillery
under the orders in forms prescribed by it.
9.124 The
licensee shall duly comply with any directions that may from time to time be
issued by the Excise Commissioner. Concerning the price or prices to be charged
by him to licensed vendors, and shall, if and whenever to directed, forthwith
reduce or enhance as the case may be, such price or prices.
9.125 No holder
of a distillery license shall sell country spirit at prices higher than those
fixed by the Excise Commissioner from time to time.
9.126 With
reference to rules 9.95 and 9.96 of these rules the following specifications of
light caoutchouchine and mineral pyridine, bases of wood naptha for use in the
denaturation of spirit which have been approved by the Excise Commissioner are
published for information.
(A) SPECIFICATION FOR LIGHT
CAOUTCHOUCINE
1.
Nature by “caoutchoucine” is meant the liquid obtained
by the dry distillation of vulcanised rubber. By “light caoutchoucine” is meant
the liquid obtained by redistilling “caoutchoucine” and correcting that portion
which passes over, at or below about 200 C.
2.
The specific gravity of light caoutchoucine. The
specific gravity of light caoutchoucine at 60 F should lie between 835 and 860
referred to water as 1.000.
3.
BOILING TEST. For the purpose of this test, 100 cc of
light caoutchoucine should be redistilled in the pyridine testing flask (see
specification for pyridine bases) Under those conditions not more than 15 cc of
distillate should pass over at or below 100 C whilst a total (including the
foregoing of at least 70 cc) should pass over at or below 200 C.
4.
ABSENCE OF SOLUBLE CONSTITUANTS: When 25 cc of light
caoutchoucince are shaken with an equal volume of water in a stopered graduated
cylinder, and due time is allowed for the liquids to separate again into two
layers, the light caoutchoucine should show no appreciable diminution in
volume.
5.
NEUTRALITY: The aqueous layer obtained from test (4)
should show no marked acidity or alkalinity when tested with both red and blue
litmus paper.
6.
LIMIT OF SATURATED HYDROCARBONS: At least 70 percent of
the light caoutcheucine should be soluble in concentrated sulphuric acid. For
testing this 25 cc should be measured off into a tapped and stopered separating
cylinder of suitable capacity and sulphuric acid should be added at first with
great care, and in very small quantities. After each addition of acid the
cylinder should be shaken and cooled to avoid loss of volatile constituents.
Sufficient acid must be used (usually about 590 cc ) for the high coloured
layer to become quite fluid so that is can separate readily from the upper
layer of unattached constituents. After a final thorough shaking and cooling
the cylinder should be left for about three hours to effect complete separation
of the two layers and the lower layer be then tapped off. The almost colourless
upper layer should be again shaken with storing suplhuric acid until it appears
free from soluble constituents (as judged by the colour imparted to the
sulphuric acid) and separated as before after standing. It should finally
measure not more than 7 cc s. The acid used should be of specific gravity 1.84
and may be of commercial quality.
7.
FREEDOM FOR WATER- Light caoutcheucien should not
contain any appreciable amount of water any officer engaged in drawing samples
for test should certify on the bottle that he has drawn the samples from the
bottom of the containing vessel, where the water, if present, will be found.
For this purpose he should employ a siphon tube of which the shorter reaches to
the floor of the containing vessel. He should also assure himself that the
sample is collected in a bottle free from moisture.
(b) SPECIFICATION FOR MINERAL PYRIDINE
BASES
I.
Colour.- The
colour must not be darker than that given by two cubic centimeters of
deci-normal iodine solution dissolved in one liter of distilled water.
II.
Miscibility With
Water.- 20 cc of the pyridine based should give a clear mixture with 40 c c
of water, or else a mixture only so slightly opalescent that, after stand for
five minutes, ordinary newspaper type is clearly visible through a layer 15 cm
deep.
III.
Amount Of Water
Present.- From 20 cc of the pyridine bases mixed with 20 cc of caustic soda
solution (density 1.4) at least 18.5 cc of the bases should separate after
having been repeatedly shaken together and allowed to stand.
IV.
Titration.-
Dissolve 1 cc of the pyridine bases in 10 cc of distilled water. Titrate with
normal sulphuric acid until a drop of the mixture give a definite blue spot on
congo-red paper (the blue colour should at once disappear). At least 10 cc of
the normal sulphuric acid should be required to produce this reaction (To
prepare the congo red paper, dissolve one gram of congo red in one liter of distilled water. Soak
filter paper in this and then dry.
V.
Cadmium
Choloride Reacton.- Vigorously shake together 10 cc of a
solution of 1 cc of pyridine bases in 100 cc of distilled
water with 5 cc of a 5
per cent solution of dry fused
Cadmium Chloride. A distinct crystalline precipitate should immediately result.
VI.
Boiling Point.-
Distil 100 cc of the pyridine bases in the manner described below. At least 90
per cent should distil, over at or under 140 degree C.
METHOD 100 cc of pyridine bases
are placed in a short necked copper flask of about 200 cc capacity. The flask
is arranged on an asbestos card, which has a circular hole of 30 m.m diameter
cut in it. To the flask is attached a fractionating column (consisting of a
tube 13 mm wide and 170 mm long, provided with one bulb) of which the side tube
(issuing 1 cm above the bulb) joins a Leibing’s condenser of which the cooled
part is at least 400 mm long. A standard thermometer is placed in the head of
the column so that its bulb occupies the center of the bulb of the column.
The speed of distillation is
adjusted to 5 cc per minute the distillate being received in a graduated
cylinder. At least 90 cc should distil over at or under 140 degree C at a barometric pressure of 760 mm.
If the barometer varies from 760
mm a correction of 1 degree C for each 30 mm of variation should be applied
(e.g under 770 mm of pressure 90 cc of distillate should come over at or under
140.3 degree C whilst under 750 mm the same amount of distillate should come
over at 139.7 degree C.
The above pattern is specified
in the German Government’s regulation and has been suggested for adoption as
being a simple form obtainable in every chemical laboratory. (Messrs Farid and
Tat Jock Ltd. have been furnished with the detail with a view to its supply).
The more modern double surface condenser may of course be substituted where
available.
(C) SPECIFICATIONS OF CRUDE WOOD
NAPTHA
(1)
Not more than 30 cubic centimeters of wood naptha
should be required to decolorize 0.5 grain of bromine.
(2)
It should be natural or slightly alkaline to litmus; 25
cubic centimetres of wood napatha should require at least 5 cubic centimeters
of N/10 acid using methyl orange as indicator.
(3)
It must contain at least 72 per cent by volume of
methyl alcohol (Methanol). In order to estimate the amount of methanol the
fractional distillation test ( Government Laboratory London) will be taken as
standard.
(4)
In 100 cubic centimeters of wood naptha there should
not be less than 5 grams of substance present (calculated as acetone), as
measured by Messinger’s test.
(5)
There should be not less than 1.5 grais of esters
present calculated as methyl acetate.
The fractional distillation test
is a as follow:-
100 cubic centrimetres of the
sample are to be slowly heated in a small copper flask fitted with a glass
fractioning column, 7 inches high and ¾ inch in diameter filled to the extent
of 4 inches of its height with small glass beads provided with a thermometer
placed opposite the exit tube glass beads provided with a thermometer placed
opposite the exit tube about an inch above the beads and that connected with a
spiral condenser. Not more than 10 cubic centimeters of distillate should be
collected in the receiver when the thermometer in the fractionating column
marks a temperature of just under 149 F. (65 C) from 80 cubic centimeters to 85
cubic centimeters should pass over between 149 F. (65C) and 162 F(72.2 C) and a
total quantity of 97 cubic centimeters to 98 cubic centimeters should have
passed over before the thermometer marks 212 F (100 C)
9.127 If the licence infringes or
causes or permits any person to infringe any of the provisions of these rules,
or any of the conditions of his license, the Collector may revoke and determine
the license and may also order the forfeiture to Govt. of the whole or any part
of the security deposit.
Provided that the revocation
of the license or forfeiture of the security may be foregone on the payment of
such sum (not exceeding the amount of security deposit) as the Collector may
deem fit to accept.
Notification No. 13-98/161-EX(P)III, dated 21st February, 1998. Excise
Commissioner, Punjab.
Notification
No.2002-2003/318-Excise & Taxation (P) dated 30.06.2003 Excise
Commissioner/Director General, Excise & Taxation, Punjab.
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